RESEARCH ON OUR SITE
 
 

ODE beamline

Research Contents > Beamlines > ODE
Description
Technical data
Scientific Opportunities Contacts
Employment    
Description

X-ray absorption spectroscopy has progressed in the last twenty years to become one of the most widely used techniques in the science of materials. It helps identify the most absorbing element while specifying its chemical state (an oxidized metal will not give the same signal as a pure metal), the number and nature of neighboring atoms as well as their distance from the excited atom.

The principle of this line, which makes it possible to focus on the sample - without having to move - the entire energy range required for the instantaneous recording of the absorption spectrum, is particularly adapted for rapid kinetics experiments (in the area of a millisecond), as well as for absorption measurements under extreme conditions of pressure and temperature. The main set of themes involves geosciences, chemical reactivity and the transitions of phases with particular emphasis on high-pressure magnetism.

 

Technical data
Energy range   3.5-25 KeV
  
Energy Resolution (∆E/E)  

7000(Si111)
25000 (Si 311)
  

Source  

Bending magnet 
 

Optics  

- under vacuum bent single crystal polychromator,
- One under vacuum 1300mm long mirror,
- One air 250 mm flat mirror.
 

Sample Environment  

- High pressure cells with low or high T: 3k to 500K
- stopped flow
- Cryostat down to 3 K
- Magnetic field up to 1.3T
 

Flux on sample  

~ 5.109 photons s-1eV-1 @ 7KeV in 25*35 μm FWHM 
 

Detectors  

- two CCD camera coupled with scintillator
- one fast Ultra DAC quantum detector (micro second )
- various X-ray camera for optics alignment
 

 
Scientific Opportunities

 
Magnetic characterization of materials by X-ray Magnetic Circular Dichroism X-ray Magnetic Circular Dichroism is a selective technique where we measure <M>, the mean value of the magnetic moment on a given atomic site. The XMCD studies that can be planned on the dispersive EXAFS beam line at SOLEIL concern characterization of bulk or nano objects, magneto-volumic effects with the combined applications of high pressure and magnetic field, high spin-low spin transitions on molecule-based magnets.
 

Materials under
extreme conditions
 

The main effect of high pressure is to reduce the interatomic distances and therefore to modify the interaction between atoms. High pressure, possibly combined with high or low temperature, is experimentally produced using diamond anvil cells. In these cells, the sample room is typically 125 μm in diameter and 20 μm in thickness. Thanks to its focusing optic, the X-ray dispersive set-up is particularly well adapted to high pressure XAS experiments.
 

Chemistry and time
resolved measurements
 

At the present time, dispersive XAFS is the unique way to collect EXAFS spectra in a sufficient photon energy range in a few μs. This is a valuable characteristic of the technique which allows to follow the kinetic of chemical reactions. Electrochemical problems or synthesis studies have been undertaken in the past and should develop in the future.
 

 
Contacts
François Baudelet
(Principal beamline scientist)
 
Tel: +33(0)1-69 35 96 12
francois.baudelet@synchrotron-soleil.fr
Qingyu Kong
(Beamline scientist)
 
Tel: +33(0)1-69 35 97 84 quingyu.kong@synchrotron-soleil.fr
Alberta Congeduti
(Beamline scientist)
 
Tel: +33(0)1-69 35 96 62 alberta.congeduti@synchrotron-soleil.fr
Lucie Nataf
(Post-doc)
 
Tel: +33(0)1-69 35 96 62 lucie.nataf@synchrotron-soleil.fr
Jean-Daniel Cafun
(Post-doc)
 
Tel: +33(0)1-69 35 81 69 jean-daniel.cafun@synchrotron-soleil.fr
Sébastien Chagnot
(Engineer assistant)
 
Tel: +33(0)1-69 35 96 50 sebastien.chagnot@synchrotron-soleil.fr
Synchrotron SOLEIL
L'orme des Merisiers
Saint-Aubin - BP 48
91192 GIF-sur-YVETTE CEDEX
Tel: +33(0)1-69 35 90 00
Fax : +33(0)1-69 35 94 56
 

 
Employment

Click here to access to the SOLEIL employment web page

 

 Beamline scientific articles
 

 News:
- Time resolved EXAFS/XANES measurements - microsecond resolution

- Studying batteries… in vivo
  
- Magnetism under extreme
condition

 
- Interplay between morphology and metallization in amorphous-amorphous transitions

 

 General information:

Preliminary Project

Notice

 Beamline poster

 Download diagram
of the energy ranges

Accueil