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SAMBA beamline
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Description
Technical data
Scientific Opportunities Contacts
Employment    

Description

SAMBA is one of the two hard X-ray absorption spectroscopy (XAS) beamlines at SOLEIL together with Diffabs. SAMBA aiming to be dedicated to large and varied scientific communities from physics to chemistry and biology, is characterised by a lot of techniques combined to XAS, such as Differential Scanning Calorimetry, Raman Spectroscopy and UV-Visible Spectroscopy. The design of SAMBA optics is optimised in order to be very versatile, to cover permanently the 4-40 keV energy range with a high flux of photon and a good energy resolution. Measurements of the absorption coefficients will be done either in the step by step mode or in a quick mode (september 2009). A SEXAFS experiment is also available at the end of the beamline.

 

Technical data
Energy range
 
  Between  4 to 40 keV
Energy Resolution
(ΔE/E)
  Si(111) : 1.2x10-4 @ 5 keV
Si(220) : 6x10-5 @ 15 keV
 
Source
 
  Bending Magnet  Radiation (Ec = 8.65 keV)  6 mrd Horizontal x 1 mrd Vertical
Flux in the XAS hutch   Si(111) : 5x10+12 Phot/s/0.1%bw @ 5 keV
Si(220) : 2.3x10+12 Phot/s/0.1%bw @ 15 keV
Si(220) : 2.3x10+11 Phot/s/0.1%bw @ 35 keV
 
Optics   Two monochromators between two bendable parabolic mirrors.

The first one is a sagittal focusing monochromator and the second one will be dedicated to quick scanning exafs acquisition mode (september 2009).
 
Sample Environment  

Many ancillary devices like cryostats (He liq and N 2liq), furnaces, thermostated liquid cells and many sample-holders.

Raman Spectroscopy

UV-Visible Spectroscopy

Differential Scanning Calorimetry

(x-ray diffraction as a further developement)

Beam size at sample
(EXAFS hutch)
 
  200x300 μm2
Beam size at sample
(SurfAs hutch)
 
  300x300 μm2
Detectors   Ionisation chambers

Multi-elements Germanium Detector

Total electron yield

Scientific Opportunities
Material science   Determination of structural and electronic properties and average size of nanosystems. Dynamic or static study of new anodic or cathodic materials. Understanding of magnetic phase transition of molecular system in coordination chemistry. Characterisation of glasses etc...
 
Physic   Investigation of clusters embedded in matrices.
 
Biology , Biomaterials   Study of reactivity of biomimetic compounds which are used as simple model compounds to understand the mechanism of catalysis of more sophisticated systems like metallo-enzymes. Investigation of metal ions present in metallo-proteins and in bio-inorganic complexes.
 
Earth and environmental sciences   Local environment probe of any element in natural systems (soils, sediments, snow, plants, microorganisms ...).
 
Surface science   Characterisation of the local structure of thin films at the very first stages of growth. Study of the interfaces : metal/metal, metal/semiconductor and oxides/metal.
 
Catalysis   Structural and electronic characterisation of catalysts in order to understand/predict their catalytic activity/selectivity in a given reaction. (DeNOx catalysis, Fischer-Tropsch, hydrogenation of hydrocarbons ...).
Beamline Status : Operationnal first trimester 2007
Contacts
Valérie Briois
(Principal beamline scientist)
 
Tel : +33(0)1-69 35 96 44
Beamline (97 23 or 97 25)
valerie.briois@synchrotron-soleil.fr
Emiliano Fonda
(Beamline scientist)
 
Tel : +33(0)1-69 35 96 33
Beamline (97 23 or 97 25)
emiliano.fonda@synchrotron-soleil.fr
Stéphanie Belin
(Beamline scientist)
 
Tel : +33(0)1-69 35 96 45
Beamline (97 23 or 97 25)
stephanie.belin@synchrotron-soleil.fr
Laurent Barthe
(Beamline assistant engineer)
 
Tel : +33(0)1-69 35 96 27
Beamline (97 23 or 97 25)
laurent.barthe@synchrotron-soleil.fr
Camille La Fontaine
(Post Doc)
Tel : +33(0)1-69 35 80 94
Beamline (97 23 or 97 25)
camille.lafontaine@synchrotron-soleil.fr
Synchrotron SOLEIL
L'Orme des Merisiers
Saint-Aubin - BP 48
91192 GIF-sur-YVETTE CEDEX
Tel : +33(0)1-69 35 90 00
Fax : +33(0)1-69 35 94 56
 
Employment

 Click here to access to the SOLEIL employment web page

 

 

Latest scientific publications

Preliminary project

Notice (in French)

 Beamline poster

Users informations

Beamline committee

 Download diagram
of the energy ranges

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